Varian NMR System 500NB 
Lilly
3 methyl Glutaric Acid
Full 22 ul 3.2 mm Rotor
Spin rate 10 kHz
16 scans, recycle = 5 s
sw=50000, at = 0.05 with 0.100 linear prediction 
no weighting or trapezoidal multiplication
CP 13C at 62.5 kHz, 1H at 72.5 kHz
Decoupling 100 kHz with SPINAL 64
pwHspinal = 5.0 us, phase = +/- 8 degrees 
