overcookedpizza
2007-12-24, 22:08
http://www.powerlabs.org/chemlabs/nmannitol.htm
Can I just replace the mannitol with erythritol in his reaction?
I'm using 70% nitric acid, and 98% sulfuric acid.
I'm not sure on how to perform this, because the reactions I found on roguesci and sciencemaddness use 99% nitric acid.
Does anyone have a tutorial, or at least some hints?
Would dissolving the erthritol in in the nitric acid and then dripping the sulfuric acid with a burret work?
How much time do I let the reaction proceed, and at what temperature should I keep it?
Also, I intend to use a magnetic stirrer, and a crushed ice/ammonium nitrate icebath.
Can I just replace the mannitol with erythritol in his reaction?
I'm using 70% nitric acid, and 98% sulfuric acid.
I'm not sure on how to perform this, because the reactions I found on roguesci and sciencemaddness use 99% nitric acid.
Does anyone have a tutorial, or at least some hints?
Would dissolving the erthritol in in the nitric acid and then dripping the sulfuric acid with a burret work?
How much time do I let the reaction proceed, and at what temperature should I keep it?
Also, I intend to use a magnetic stirrer, and a crushed ice/ammonium nitrate icebath.