Could you look up the solubility of DMT HCl in water (acidic water) and the solubility of the freebase in xylene or other nonpolar solvents?? That would be amazing....

I'm not sure about the HCl, but the freebase is roughly 1 gram per 30 ml of hot naptha.

Free online Merck Index: https://themerckindex.cambridgesoft.com/TheMerckIndex/default.asp?formgroup=basenp_form_group&dataaction=db&dbname=TheMerckIndex
enjoy;)

seems to need a subscription...

seems to need a subscription...

lulz... forgot about that, only had to login once. Try one of these http://www.bugmenot.com/view/cambridgesoft.com

Logging in isn't the problem - you can set up a free account.

The database actually needs a subscription...

Logging in isn't the problem - you can set up a free account.

The database actually needs a subscription...

I regularly use that site, and I just logged on with one of the passwords on bugmenot. I don't remember exactly where I entered it, but now I have free access to the Merck Index 14th ed.

From sciencemadness

Link for Merck Index 14th ED

* Publisher: Merck
* Number Of Pages: 2564
* Publication Date: 2006-11-03
* ISBN-10 / ASIN: 091191000X
* ISBN-13 / EAN: 9780911910001
* Binding: Hardcover


Code:
http://ifile.it/42jgesx
http://ifile.it/0a8xpvz
http://ifile.it/18edrlm
http://ifile.it/3e62c0m
http://ifile.it/08uq5ck
Serial: 311-324285-8925
Activation code: EYT-QQ7EI-7Z-S54H-7Z7G2-74H7-ZPGQL
Props to the member anoopai

EDIT: Other members seem to be having trouble getting it to activate. If you go on SM in the references forum there is a thread with like 20 links to Indexes 12, 13 and 14.

Could you look up the solubility of DMT HCl in water (acidic water) and the solubility of the freebase in xylene or other nonpolar solvents?? That would be amazing....

I just realized no one answered your question yet, sorry about that!

Monograph number: 03262
Title: N,N-Dimethyltryptamine
CAS Registry Number: 61-50-7
CAS Name: N,N-Dimethyl-1H-indole-3-ethanamine
Additional Names: 3-[2-(dimethylamino)ethyl]indole; DMT
Molecular Formula: C12H16N2
Molecular Weight: 188.27
Percent Composition: C 76.55%, H 8.57%, N 14.88%
Literature References: Occurs naturally in plants with hallucinogenic properties. Isoln from the leaves of Prestonia amazonica (Benth.) Macbride (Haemadictyon amazonicum Spruce & Benth.), Apocynaceae: Hockstein, Paradies, J. Am. Chem. Soc. 79, 5735 (1957). Metabolism: St. Szára, Experientia 12, 441 (1956); B. R. Sitaram et al., Biochem. Pharmacol. 36, 1509 (1987). Relationship between hallucinogenic activity and electronic configuration: Snyder, Merril, Proc. Natl. Acad. Sci. USA 54, 258 (1965). Synthesis: I. Fleming, M. Woolias, J. Chem. Soc. Perkin Trans. 1 1979, 829. Differential interaction with serotonin receptor subtypes: A. V. Deliganis et al., Biochem. Pharmacol. 41, 1739 (1991). Fluorometric detection: O. Jules et al., Anal. Chim. Acta 169, 355 (1985). Review of biosynthesis, metabolism and bioactivity: S. A. Barker et al., Int. Rev. Neurobiol. 22, 83-110 (1981).
Properties: Crystals, mp 44.6-46.8°; also reported as plates from ethanol and light petroleum, mp 46° (Fleming, Woolias). bp 60-80°. pKa 8.68 (ethanol-water). Freely sol in dil acetic and dil mineral acids.
Derivative Type: Methiodide
Properties: mp 216-217°.
Note: This is a controlled substance (hallucinogen): 21 CFR, 1308.11.

That's all they have online :(

Well damn. I was hoping for more info on the freebase in nonpolars... I've heard 1g is freely soluble in 100mL naphtha at RT but that's all i've got.
Now, freely soluble in acetic/mineral acids means that a litre of pH 2 HCl/water soln. will easily dissolve 10g, correct?
Also this is really basic, but i got kicked out of school before we did equilibrium and had to teach myself... pKa refers to equilibrium, correct?
Last one- what are your all's thoughts on freebasing DMT out of a water solution and filtering, using ammonia

Well damn. I was hoping for more info on the freebase in nonpolars... I've heard 1g is freely soluble in 100mL naphtha at RT but that's all i've got.
Now, freely soluble in acetic/mineral acids means that a litre of pH 2 HCl/water soln. will easily dissolve 10g, correct?
Also this is really basic, but i got kicked out of school before we did equilibrium and had to teach myself... pKa refers to equilibrium, correct?
Last one- what are your all's thoughts on freebasing DMT out of a water solution and filtering, using ammonia

1) Ammonia wash
2) Ice cold DH2O wash (vac filtered)
3) Recrystallized from boiling methanol
4) Consume :)